This blog focuses on industrial, inline process refractometers and their use in industrial applications. Refractometry is used to measure the refractive index of a substance in order to determine its composition or purity. Posts include information on theory, construction, installation, new products and new markets.
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Inline Process Refractometers for Industry
Inline Process Refractometers in Sugar Cane Processing
- Product flow is adapted to evaporator capacity to save energy.
- Extraction process optimization, reducing the amount of water at the evaporator.
- Feed juice control in the separation column to modify concentration to meet capacity.
- Check for quality assurance on liquid bulk sugar and molasses.
- Automatic and precise seeding in a vacuum pan.
- Supersaturation monitoring during the whole strike of crystallization.
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Electron Machine Corporation
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Inline Process Refractometer in Large Scale Juice Concentrate Production
The MPR E-Scan™
Inline, Realtime Analysis of Degrees Brix (°Bx) in Beverage Production
The beverage sector creates widely consumed goods while adhering to stringent quality standards. Producers of beverages are responsible for ensuring adequate quality and meet rising customer demands for innovative and consistent flavor. Reliable process control tools are required to make production viable and sustainable and maintain the highest levels of product quality. In this age of sophisticated technologies, it's essential for best practice manufacturing standards.
The degree of Brix (°Bx) indicates the amount of sugar in an aqueous solution. One degree Brix equals one gram of sucrose in 100 grams of solution and suggests the solution's strength as a percentage of mass. Brix monitoring and measurement are critical for various beverages, whether dairy, brewery, wine, soft drinks, or fruit juices.
In the beverage and juice industry, syrups and concentrates are blended with water, or fermented, according to specific recipes, stored in stacking tanks, and finally filled into product-specific bottles or containers. A standard method for Brix testing is a manual process done in a remote lab with samples taken from the process. If a primary component, such as a juice concentrate, does not precisely meet the specifications, or if the blending process itself is incorrect due to incorrect flow control, the entire production run may be flawed. Cross-contamination is another concern. If a wrong product is mixed and bottled due to a poorly controlled phase transition, rejection of the whole batch is the outcome.
The inline refractometer (a robust process control instrument) provides a highly reliable and precise measure of Brix in beverage production. Inline process refractometers are installed in the process piping and continuously measure the Brix value, constantly measuring the definition and differentiation of each product, component, juice, or beverage.
The advantages are clear for choosing inline refractometers. The time-consuming and labor-intensive manual sampling and laboratory analysis are less efficient and less repeatable. The more efficient and reliable solution is the inline process refractometer. These devices offer real-time, inline continuous concentration measurement and cross-contamination protection. Additionally, operators can use their time to perform other critical activities, enabling other time-savings quality improvements.
Electron Machine Corporation
https://electronmachine.com
+1 352-669-3101
MPR E-Scan™ - The World's Most Rugged In-line Process Refractometer
Inline Process Refractometers for Brewers
Beer brewing and branding are all about consistency. Process monitoring is thus vital. With Electron Machine inline refractometers, you'll have less waste, use less energy, spend less money, and achieve better beer.
While some breweries still use manual sampling and lab analysis, the trend is adapting inline monitoring and automation. Laboratory analysis is part of R&D. It reveals how different substances or methods affect qualities like flavor and fragrance. Laboratory analysis is vital in research as it provides an understanding of chemistry. However, the utility of sampling and analysis can be limited in manufacturing due to costs and delays when the lab findings indicate the issue. Slow sample timing results in possible lost production and waste. Similarly, because the sample is a snapshot of the process, it cannot provide feedback control, timely alarms, or indicate trends.
The angle of refraction of light in the process medium determines the refractive index (RI), which the inline refractometer computes important process variables continually. Electron Machine inline process refractometers will calibrate to Brix, Gravity, Density, or Plato and withstand CIP/SIP cleaning and rinsing operations.
Process refractometers have a quick response time which provides critical information in all stages of beer production. Examples of applications for inline refractometers that arise throughout the brewing process:
- Grain mashing - Refractometers measure mash concentration in the output pipe water.
- Lautering - While the spray water rinses the grains, it completes the sugar extraction process and produces clear wort. The refractometer continuously measures this concentration to determine the rinsing breakpoint, saving water and electricity.
- Wort boiling - Refractometer installed directly on the wort boiler continuously measures wort strength / specific gravity, allowing the brewer to determine the required concentration.
- Rousing or Swirling - Solid particles are removed from the bitter wort in a vortex. The vortex causes the leftover particles to thicken and form sludge. The solids removal uses refractometers placed before or after the vortex for a clear bitter wort for the next phase.
- Cooldown - A heat exchanger cools the wort, recovering some of the energy needed to boil it. Refractometers are affixed to the cooler's outflow to ensure the bitter wort has the proper level of dissolved solids.
- Fermentation - Yeast ferments wort to produce CO2 and alcohol. The specific gravity (or relative density) of the fermented liquor is determined using refractometers. The alcohol concentration directly correlates between the initial wort density and current density, so the refractometer can closely monitor fermentation. It gives brewers real-time information into the process, allowing them to predict fermentation completion.
- Filtration and Aging - The beer is rested after fermentation to settle the used yeast. But several filtration procedures are used to refine the beer as the last chance to impact beer quality. Refractometers assist in measuring bitterness, flavor, fragrance, foam stability, clarity, alcohol, and gas percentage.
- Filling and CIP (Clean-in-Place) - With the refractometer, you can quickly swap between items or batches and easily detect production from cleaning products.
In summary, refractometers assist brewers in optimizing processes, decreasing waste, saving energy, and maintaining consistency, and making great beer.
Electron Machine
352-669-3101
Ensure Juice and Beverage Quality and Consistency with Inline Process Refractometers
Inline refractometers also assure that the correct product is in process, particularly when blending and filling a variety of juices, syrups, nectars, soft drinks, and other beverages on the same line.
Syrups, juice concentrates, and other ingredients are frequently blended with water according to specific formulas, then held in stacking tanks, and lastly poured into product-specific bottles or containers in the beverage industry.
The entire product batch may be defective if a primary component, such as a juice concentrate, does not precisely meet the specifications or if the blending process itself is incorrect due to incorrect valve switching. It's also possible that the faulty product goes to packaging due to an improper phase transition. If this is discovered only during final quality control, the entire production batch could be at risk.
With an inline refractometer, each process stage gets precisely managed by measuring the dissolved sugar in the liquid. In comparison, manual Brix control sampling with a hand refractometer is labor-intensive and open to operator error. Furthermore, any mistake can only be detected after the fact, affecting the production quantity between two samples or a complete filling batch, and then discarded. The inline process refractometer is integrated directly into the process with high accuracy and continuously, allowing the definition and differentiation of each component or product.
Contact Electron Machine Company at +1 352-669-3101 or visit https://electronmachine.com if you have any question regarding the usage of refractometry in food and beverage production.
Green Liquor Process Management with Inline Refractometers
Green liquor is the dissolved concentrations of sodium sulfide, sodium carbonate, and other substances from the paper-making process's recovery boiler. Measuring its density is an essential aspect of paper production quality.
The Electron Machine MPR EScan is used to measure the green liquor dissolved density, or TTA, at two different points in the process: after the green liquor dissolving tank and after the green liquor clarifier. With the refractometer sensing head positioned directly in the primary process lines, inline measurement enables real-time management of green liquor dilution to meet target TTA set-points. Excessive green liquid density and the accompanying harmful imminent crystallization within the dissolving tank are also indicated (and prevented) by the measurement.
One considerable challenge is sensor head scaling associated with green liquor. An optical coating forms on the refractometer sensing head. The coating must be dealt with efficiently and quickly to maintain the accuracy and with minimum maintenance. This is key for the refractometer's ability to provide an acceptable measurement cycle and duration. The maintenance necessary to keep the cleaning system running efficiently is challenging.
Controlling scaling is optimal when the variance of green liquor solids is reduced by automatically adjusting weak-wash dilution with the MPR E-Scan refractometer. Additionally, pressurized water, heated to the process temperature, rinses the refractometer optical components effectively, resulting in a further scaling reduction. The end outcome is advantageous for both control and acceptable maintenance scheduling.
By limiting thermal changes, minimizing maintenance, and providing a dependable measurement source for automatic inline control, refractometers with accompanying heated high-pressure water cleaning systems deliver excellent results in improving green liquor processing.
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Automatic Black Liquor Solids Content Measurement with Inline Refractometers
Until the early twentieth century, when recovery boilers first appeared, black liquor was a disposable by-product in paper production. In modern times, pulp mills use chemical recovery technologies to recapture spent cooking chemicals from the pulping process for economic and environmental reasons. An example is Black Liquor Recovery Boilers that enable papermakers to recover and reuse inorganic compounds while also extracting energy from pulping leftovers.
The Kraft process is used in paper production, in which wood is transformed into wood pulp and ultimately into paper. However, the method generates a byproduct known as black liquor, a hazardous mixture of pulping wastes (such as lignin and hemicellulose), and inorganic Kraft process chemicals (such as sodium hydroxide and sodium sulfide). The weak black liquor is directed through evaporators to increase the solids content to form strong black liquor. Injection of the concentrated black liquor into the recovery furnace burns organic molecules and reduces Na2SO4 to Na2S. The high energy content of the black liquor burned in the recovery furnace recovers as steam for process requirements such as boiling wood chips, heating, evaporating black liquor, preheating combustion air, and drying the pulp or paper products.
The pulp industry places a high value on accurate, continuous measurement of black liquor solids concentration. Black liquor solid is an essential measurement operation influencing the economics of the pulping process. The mill's environmental load and the solids content of liquor injected into a recovery furnace can significantly impact the firing behavior and thus efficiency. Current trends toward better recovery furnace control for safety and lower air emissions necessitate more robust control over incoming solids content and proper modification of operating parameters to accommodate changes in solids content. Typical analyses of black liquor solids are conducted periodically throughout the mill, from the washers through the evaporator to the ring header. These analyses consist of taking many samples at critical locations and analyzed in the lab. Alternatively, as pulp and paper mills are modernized and automated, inline process refractometers are installed, providing dependable, accurate, and reliable solids measurement and contributing to the safe functioning of recovery boilers. Inline process refractometers are time-tested and proven to provide reliable and precise automatic monitoring of black liquor solids concentration and providing considerable time and labor savings.
For more information about inline process refractometers for black liquor processes visit this link or contact Electron Machine at 352-669-3101.
Industrial Applications for Inline Refractometers
The applications for inline industrial refractometers are many. Outlined below are several of the more common applications and processes.
Spray Dryers: Spray drying is a way to produce a dry powder from a liquid or slurry by drying quickly with a warm gas, a preferred drying technique for many thermally sensitive products like foods and pharmaceuticals. Consistent distribution of particle size is the goal for spray drying. Process refractometer monitors the feed line's concentration to the spray dryer, ensuring correct particle size after drying and improving product shelf life.
Evaporation: An evaporator is a tool used to transform the liquid form of a chemical substance such as water into its gaseous / vapor form. During that phase, the liquid is evaporated or vaporized into a gas. Inline refractometers provide real-time data of concentration changes in the process media.
Crystallizers: In industry, crystallizers create liquid-solid separation. They are an essential component of chemical processing equipment as they can generate high-purity products from a relatively low energy input. The refractometer controls the liquor concentration to determine the right seeding point (evaporative crystallizer) or to detect when crystals start to form (cooling crystallizer).
Dissolving Tanks: Dissolving tanks dissolve solids into a liquid, thereby changing the concentration of the solution. Refractometers provide continuous measurement of the concentration components in solution as the solute dissolves into water or solvent, with real-time information for dissolving rate.
Solid / Liquid Extraction - Solid / Liquid extraction method is a prevalent method in the pharmaceutical, cosmetic, and food industries to acquire natural ingredients such as natural raw material flavors and fragrances. Inline refractometers measure the amount of extracted substance (dissolved solids) in the liquid after the extraction process. The measurement is not affected by undissolved solids, only by the dissolved matter, making it ideal to follow extraction efficiency.
Reverse Osmosis: Reverse osmosis (RO) is a water purification method that removes ions, unwanted molecules, and bigger particles from drinking water using a partially permeable membrane. Inline refractometers provide real-time data of concentration changes in the process media.
Reactors: Process reactors are typical in commercial production applications in adhesives processing, agriculture, chemical processing, cosmetics, food and beverage production, paints and coating production, paper and pulp processing, pharmaceutical and medical production, plastics, and thermoplastics processing. The real-time progress can be followed using inline refractometers, either through the leveling out of process key process variables or reaching a single component's targeted refractive index value.
Cooking Processes: The art, technology, science, and craftsmanship of preparing food for consumption are cooking. The large-scale production of juices, jams, jellies, dairy, and fruits in modern production facilities requires automation and control instrumentation for quality and efficiency. Sugar is a critical component in many foods. The inline refractometer measures the refractive index to determine the cooking process's end and boost the cooking effectiveness.
Other areas where you'll find the use of industrial process refractometers are; adhesives processing, agriculture, chemical processing, cosmetics, food and beverage production, paints and coating production, paper and pulp processing, pharmaceutical, plastics, and thermoplastics processing.
For more information about applying the refractive index to industrial process applications, contact Electron Machine by calling 352-669-3101 or by visiting https://electronmachine.com.
Demonstration of Measuring °Brix in Soft Drinks (Soda) with an Inline Process Refractometer
Are you a soda manufacturer that wants better quality control while reducing cost? Stay tuned to see how the inline process refractometer can help you out.
Welcome to Electron Machine Corporation, manufacturer of the world's most rugged refractometer, found in various industries across the globe.
The next series of videos will highlight some of the most common applications for Electron Machine refractometers.
Typically installed in a pipeline, the MPR E-Scan is set up here as a demonstration equipment piece. In this demo, a static cup measures a variety of popular sodas. The refractometer s commonly installed either on a bottling line to determine what soda you're running or on the blending line mixing the syrup with the carbonated water to ensure that it stays at the correct consistency from bottle to bottle.
Hopefully, you'll enjoy this quick little look into what the refractometer actually can do and how it measures orange juice. Stay tuned for the next series of videos. We'll highlight another product for the refractometer to measure.
Electron Machine Corporation
https://electronmachine.com
+1 352-669-3101
Improve Your Food Production Process with Continuous, Inline Process Refractometers
Adherence to the concentration of dissolved substances in food production is crucial for consistent product quality. Using a refractive index measuring instrument called a refractometer is an excellent method to monitor these concentrations.
Refractometers measure the magnitude of redirection light when immersed in a fluid, referred to as the angle of refraction. The refractometer takes these measurements and correlates them to the refractive index (nD) - a long-established calculation of known values. These values determine the concentrations of the solutions.
Measuring the dissolved solids in food production offers enormous potential for increased efficiency and quality. In many applications, the process is manual, whereby measurements are done by hand repetitively and at short intervals. This is disruptive to the process and slow. A much more efficient and time-saving way is by taking process measurements with a pipe mounted (inline) continuous refractometer, such as the Electron Machine MPR E-Scan.
The density of the liquid varies as the number of dissolved particles increases or decreases. The MPR E-Scan continuously monitors the concentration using an inline sensor, enabling accurate measuring of the devolved solids, enabling repeatable management of the process. Typical applications run the gamut in all aspects of the food industry. Examples in food production include control of sugar concentration of juices, soft drinks, jams, jellies; measuring the milk fat solids in dairy products; and mash measurements, wort concentration, and alcohol level. By taking measurements continually and in real-time, production run time are shortened and efficiency is dramatically increased.
Electron Machine Corporation
https://electronmachine.com
+1 352-669-3101
Check out our latest Ad in PI Process Instrumentation Magazine!
Electron Machine is pleased to be advertising in PI Process Instrumentation Magazine. P.I. Process Instrumentation (formerly named Flow Control).
Inline Process Refractometers from Electron Machine
As the pioneer in developing the industrial use of refractive index, Electron Machine’s instruments provide safe, reliable, and accurate process measurement for the pulp and paper industry, the food and beverage industry, and the chemical industry. With thousands of refractometers installed around the world, Electron Machine sells and supports it products through its Umatilla, Florida headquarters and a global network of technical distributors.
Electron Machine Corporation
https://electronmachine.com
+1 352-669-3101
sales@electronmachine.com
Inline Process Refractometers Used in Industry
Inline process refractometers are used in a wide variety of industrial and commercial applications including the measurement of the sugar content of food and beverages, monitoring the purity and concentration of ingredients in pharmaceuticals, analyzing the constituents in chemical used in pulp and paper processing, and purity control and concentration measurement of raw materials in the chemical industry.
Inline process refractometers provide a very reliable and accurate real time measurement, which is ideal for process loop optimization and control. With In-line process refractometers, product quality and batch times are more closely controlled, reducing costs as a result.
The Electron Machine Corporation has been designing and manufacturing in-line process refractometers since the early 1960s, with a focus on providing simple, rugged, and reliable instruments that provide value over time, with accurate measurement, minimal maintenance, and long service life. They are the pioneer in developing the industrial use of refractive index for safe, reliable, and accurate process measurement and control.
Electron Machine Corporation
https://electronmachine.com
352-669-3101
Inline Process Refractometers for Food & Beverage
Inline Process Refractometer Application Engineering Data: Heavy Black Liquor
As quoted from the Black Liquor Recovery Boiler Advisory Committee, “Refractometers have proven to be effective for black liquor recovery boiler service.” Refractometers are a critical component of the black liquor safe firing system.
Monitoring the recovery boiler firing liquor concentration requires two refractometers in a redundant and specially supervised system. A “Monitor Divert System” employs supervisory circuitry to oversee the correct operation of the refractometer and perform certain logic functions if it detects a failure. The most important of these is the automatic
diversion of the liquor from the furnace into a recirculation loop until the problems can be resolved.
Refractometers used elsewhere in this area include measuring the concentration of the heavy black liquor from storage as it enters the recovery area. They are also used extensively around the cascade or cyclone evaporators to monitor the performance of the direct contact evaporation system. When refractometers are used in the recovery area, the process can be tuned to operate efficiently and most importantly, more safely.
Inline process refractometer on black liquor service. |
What Is An Inline Process Refractometer?
Inline sensing head |
Inline process refractometers are made up of three main components:
Control console |
- The inline sensing head, which is inserted to a pipe and is exposed the the product for direct measurement. The sensor is connected by a cable to the second main component, the control console.
- The control console, which houses the display, electronics, power supply and output connections. Both the sensor and the control module are designed for high accuracy and precise control. Their housing and cabling are often specialized for use in varying extreme conditions and very demanding environments.
- The process adapter, which connects the sensor mechanically to the process piping. Adapters are configured for the pipe size and application they are used on and are available in many configurations. Some of the more common adapter options are:
- Lined - For extremely corrosive applications.
Mounting adapters - Inline - For most applications with pipeline sizes less than 2”.
- Isolation - For critical process lines that cannot normally be shut down.
- Sanitary - For applications on a sanitary pipeline.
- Spool - For most applications with pipeline sizes greater than 2”.
- Vessel - For applications where the sensing head is to be mounted directly onto a vessel or vacuum pan.
- Weld-in - For economical mounting.